Modular LIBS System


LIBS (Laser Induced Breakdown Spectroscopy) is a sophisticated analytical technique that involves the use of ultra-short pulse lasers to focus on the surface of a sample, creating plasma. This plasma, a highly energized form of matter, emits light that is characteristic of the elements present in the sample. By analyzing this emitted light spectrum with a spectrometer, LIBS systems can identify the elemental composition of the sample. This process allows for the identification, classification, qualitative, and quantitative analysis of materials.

LIBS (Laser Induced Breakdown Spectroscopy) is a sophisticated analytical technique that involves the use of ultra-short pulse lasers to focus on the surface of a sample, creating plasma. This plasma, a highly energized form of matter, emits light that is characteristic of the elements present in the sample. By analyzing this emitted light spectrum with a spectrometer, LIBS systems can identify the elemental composition of the sample. This process allows for the identification, classification, qualitative, and quantitative analysis of materials.

Product Introduction

The iSpec-LIBS400 Split-Type LIBS (Laser Induced Breakdown Spectroscopy) System is a versatile and sophisticated assembly tailored for scientific research, optical application experiments, and optical application centers. This system's design is particularly flexible due to its split-type configuration, allowing users to conveniently choose and configure various lasers and spectrometers to suit specific needs.

LIBS Application’s Principle 

Main Application

Coal Quality Analysis and Combustion Products Analysis

● Online Component Analysis in Metallurgical Industry

● Mineral Exploration: Online Ore Quality Analysis

● Soil Heavy Metal Analysis, Biomaterials, Aerosols, Nanoparticles

● Nuclear Materials, Waste, Petroleum Products

● Building Materials, Archaeology, Casting, Gold and Jewelry Testing

The detection limits of LIBS largely depend on the type of sample being analyzed, the specific elements being measured, and the configuration of the laser/spectrometer in the instrument. Typically, LIBS can achieve detection limits ranging from a few parts per million (ppm) to percentage levels. For most elements in common applications, the detection limit can be between 10 ppm to 100 ppm. In quantitative analysis, the relative standard deviation of measurements obtained through LIBS can be within 3-5% for most materials, and even less than 1% for homogeneous materials.

Typical Detection Limits with LIBS

● Elements like Li, Be, B, Na, Mg, Al, K, Ca: >10 ppm (0.001%)

● Elements like Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Mo: >100 ppm (0.01%)

● Elements like C, N, O, P, Si: >200 ppm (0.02%)

● Elements like F, Cl, Br, S: >0.5%

The iSpec-LIBS400 Split-Type LIBS (Laser Induced Breakdown Spectroscopy) System is a versatile and sophisticated assembly tailored for scientific research, optical application experiments, and optical application centers. This system's design is particularly flexible due to its split-type configuration, allowing users to conveniently choose and configure various lasers and spectrometers to suit specific needs.

LIBS Application’s Principle 

Main Application

Coal Quality Analysis and Combustion Products Analysis

● Online Component Analysis in Metallurgical Industry

● Mineral Exploration: Online Ore Quality Analysis

● Soil Heavy Metal Analysis, Biomaterials, Aerosols, Nanoparticles

● Nuclear Materials, Waste, Petroleum Products

● Building Materials, Archaeology, Casting, Gold and Jewelry Testing

The detection limits of LIBS largely depend on the type of sample being analyzed, the specific elements being measured, and the configuration of the laser/spectrometer in the instrument. Typically, LIBS can achieve detection limits ranging from a few parts per million (ppm) to percentage levels. For most elements in common applications, the detection limit can be between 10 ppm to 100 ppm. In quantitative analysis, the relative standard deviation of measurements obtained through LIBS can be within 3-5% for most materials, and even less than 1% for homogeneous materials.

Typical Detection Limits with LIBS

● Elements like Li, Be, B, Na, Mg, Al, K, Ca: >10 ppm (0.001%)

● Elements like Ti, V, Cr, Mn, Fe, Co, Ni, Cu, Zn, Mo: >100 ppm (0.01%)

● Elements like C, N, O, P, Si: >200 ppm (0.02%)

● Elements like F, Cl, Br, S: >0.5%

Product Features and Advantages

● Wide Range of Element Analysis: Capable of analyzing light elements (like C, H, O, N, Li, Be, B) and heavy elements, including almost all metals and non-metals.

● Integrated LIBS System: Includes a laser, spectrometer, LIBS optical collection system, a 3D sample stage with linked control system, and a dual camera imaging system.

● Intelligent Spectral Collection and Analysis Software: For peak matching, online element concentration prediction, and quantitative analysis modeling (peak height method, peak area method, etc.).

● Fast Analysis Time: A few seconds to minutes.

● Minimal Sample Preparation: Analyzes solid samples, even powders (or binders or adhesives).

● Eco-Friendly and Safe: No reaction reagents required.

● Microscopic to Macroscopic Analysis: Directed and flexible point analysis.

● Qualitative and Quantitative Analysis: Sample classification and elemental concentration.

● Multiple Laser and Probe Options: To suit different needs.

● Detection Limits: Most elements have detection limits ranging from 10 ppm to several dozen ppm.

Product Features and Advantages

● Wide Range of Element Analysis: Capable of analyzing light elements (like C, H, O, N, Li, Be, B) and heavy elements, including almost all metals and non-metals.

● Integrated LIBS System: Includes a laser, spectrometer, LIBS optical collection system, a 3D sample stage with linked control system, and a dual camera imaging system.

● Intelligent Spectral Collection and Analysis Software: For peak matching, online element concentration prediction, and quantitative analysis modeling (peak height method, peak area method, etc.).

● Fast Analysis Time: A few seconds to minutes.

● Minimal Sample Preparation: Analyzes solid samples, even powders (or binders or adhesives).

● Eco-Friendly and Safe: No reaction reagents required.

● Microscopic to Macroscopic Analysis: Directed and flexible point analysis.

● Qualitative and Quantitative Analysis: Sample classification and elemental concentration.

● Multiple Laser and Probe Options: To suit different needs.

● Detection Limits: Most elements have detection limits ranging from 10 ppm to several dozen ppm.

Filed Working

 

Filed Working

 

Main Technical Indicators

Model

iSpec-LIBS400

Element Measurement Range

Capable of analyzing elements with atomic numbers Z≥1, including organic elements such as Carbon (C), Hydrogen (H), Oxygen (O), and light elements like Nitrogen (N), Lithium (Li), Beryllium (Be), Boron (B), as well as almost all metals and non-metals.

Concentration Range

From 10 parts per million (ppm) to percentage levels, depending on the element and the configuration of the instrument.

Analysis Time

30S

Analysis Type

Both qualitative (identifying what elements are present) and quantitative (determining the concentration of each element) analysis.

Spectrometer

Four-channel spectrometer with a wavelength range of λ = 190 -820nm and a resolution of 0.2nm.

Eight-channel spectrometer with a wavelength range of λ = 190- 1070nm and a resolution of 0.1nm.

Laser

Nd-YAG laser with options for 266nm wavelength at 50mJ per pulse or 1064nm wavelength at 100-200 mJ per pulse, 10Hz frequency, 5 -10ns pulse width, equipped with a water-cooling system.

Sample Window and Positioning

XYZ three-axis fully automatic positioning sample stage, with a travel range of up to 5cm.

Stepper motor-driven, offering a positioning accuracy of 5 µm.

Sample Imaging

Dual lens configuration with a 5x wide-angle lens for broad field observation and a 400x high magnification lens for precise micro-positioning. Includes LED lighting.

Analysis Spot Size

Minimum focused spot size of 25µm.

LIBS Spectral Software

LIBS spectral data collection software, which allows control of various parameters including the sample stage, laser, focusing, and imaging, as well as other adjustments and control operations.

 

Main Technical Indicators

Model

iSpec-LIBS400

Element Measurement Range

Capable of analyzing elements with atomic numbers Z≥1, including organic elements such as Carbon (C), Hydrogen (H), Oxygen (O), and light elements like Nitrogen (N), Lithium (Li), Beryllium (Be), Boron (B), as well as almost all metals and non-metals.

Concentration Range

From 10 parts per million (ppm) to percentage levels, depending on the element and the configuration of the instrument.

Analysis Time

30S

Analysis Type

Both qualitative (identifying what elements are present) and quantitative (determining the concentration of each element) analysis.

Spectrometer

Four-channel spectrometer with a wavelength range of λ = 190 -820nm and a resolution of 0.2nm.

Eight-channel spectrometer with a wavelength range of λ = 190- 1070nm and a resolution of 0.1nm.

Laser

Nd-YAG laser with options for 266nm wavelength at 50mJ per pulse or 1064nm wavelength at 100-200 mJ per pulse, 10Hz frequency, 5 -10ns pulse width, equipped with a water-cooling system.

Sample Window and Positioning

XYZ three-axis fully automatic positioning sample stage, with a travel range of up to 5cm.

Stepper motor-driven, offering a positioning accuracy of 5 µm.

Sample Imaging

Dual lens configuration with a 5x wide-angle lens for broad field observation and a 400x high magnification lens for precise micro-positioning. Includes LED lighting.

Analysis Spot Size

Minimum focused spot size of 25µm.

LIBS Spectral Software

LIBS spectral data collection software, which allows control of various parameters including the sample stage, laser, focusing, and imaging, as well as other adjustments and control operations.

 


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